Synthesis of novel trichloromethyl substituted azolo[1,3,5]triazines
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Authors
Kalinin, D.
Kalinina, S.
Dolzhenko, Anton
Date
2012Type
Journal Article
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Kalinin, Dmitrii and Kalinina, Svetlana and Dolzhenko, Anton. 2012. Synthesis of novel trichloromethyl substituted azolo[1,3,5]triazines. Heterocycles. 85 (10): pp. 2515-2522.
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Heterocycles
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Abstract
The triazine ring bearing a trichloromethyl group was annelated to various aminoazoles using a new effective synthetic procedure. The method of preparation involved initial formation of trichloroacetamidines in the reaction of aminoazoles with trichloroacetonitrile followed by the triazine ring closure with triethyl orthoformate affording therefore the titled compounds.