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    Optimization of click chemistry of ferrocene derivatives on acetylene-functionalized silicon(100) surfaces

    Access Status
    Fulltext not available
    Authors
    Ciampi, Simone
    Le Saux, G.
    Harper, J.
    Gooding, J.
    Date
    2008
    Type
    Journal Article
    
    Metadata
    Show full item record
    Citation
    Ciampi, S. and Le Saux, G. and Harper, J. and Gooding, J. 2008. Optimization of click chemistry of ferrocene derivatives on acetylene-functionalized silicon(100) surfaces. Electroanalysis. 20 (14): pp. 1513-1519.
    Source Title
    Electroanalysis
    DOI
    10.1002/elan.200804241
    ISSN
    1040-0397
    School
    Nanochemistry Research Institute
    URI
    http://hdl.handle.net/20.500.11937/17838
    Collection
    • Curtin Research Publications
    Abstract

    The optimization of the reaction conditions for copper-catalyzed azide-alkyne ,click- cyclo-addition reactions used to covalently confine substituted ferrocene derivatives on passivated silicon(100) surfaces is reported. Variations in the observed reaction yields and the extent of surface contamination as a function of the source of the copper catalyst and the solvent system used in the ,click- procedure were evaluated spectroscopically. The electronic communication between the ferrocene centre and the underlying semiconductor surface was investigated by means of cyclic voltammetry and found to be consistent with that expected for a well-behaved and robust redox interface. © 2008 Wiley-VCH Verlag GmbH&Co. KGaA.

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