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dc.contributor.authorHumphries, Terry
dc.contributor.authorBirkmire, D.
dc.contributor.authorHauback, B.
dc.contributor.authorSean McGrady, G.
dc.contributor.authorJensen, C.
dc.date.accessioned2017-01-30T13:01:57Z
dc.date.available2017-01-30T13:01:57Z
dc.date.created2015-10-29T04:09:52Z
dc.date.issued2013
dc.identifier.citationHumphries, T. and Birkmire, D. and Hauback, B. and Sean McGrady, G. and Jensen, C. 2013. In situ high pressure NMR study of the direct synthesis of NaAlH 4 . Physical Chemistry Chemical Physics. 15 (17): pp. 6179-6181.
dc.identifier.urihttp://hdl.handle.net/20.500.11937/27922
dc.identifier.doi10.1039/c3cp50777g
dc.description.abstract

The direct synthesis of NaAlH4 has been studied, for the first time, by in situ27Al and 23Na wide-line NMR spectroscopy using high pressure NMR apparatus. Na3AlH6 formation is observed within two minutes of hydrogen addition, while NaAlH4 is detected after a total of four minutes. This indicates the formation of the hexahydride does not proceed to completion before the formation of the tetrahydride ensues. © 2013 the Owner Societies.

dc.titleIn situ high pressure NMR study of the direct synthesis of NaAlH 4
dc.typeJournal Article
dcterms.source.volume15
dcterms.source.number17
dcterms.source.startPage6179
dcterms.source.endPage6181
dcterms.source.issn1463-9076
dcterms.source.titlePhysical Chemistry Chemical Physics
curtin.departmentDepartment of Physics and Astronomy
curtin.accessStatusFulltext not available


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