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    Reverse microemulsion synthesis of monodispersed square-shaped SnO2 nanocrystals

    Access Status
    Fulltext not available
    Authors
    Yu, C.
    Zhou, W.
    Yang, K.
    Li, L.
    Chao, F.
    Li, Xin Yong
    Date
    2010
    Type
    Journal Article
    
    Metadata
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    Citation
    Yu, C. and Zhou, W. and Yang, K. and Li, L. and Chao, F. and Li, X.Y. 2010. Reverse microemulsion synthesis of monodispersed square-shaped SnO2 nanocrystals. Wuji Cailiao Xuebao/Journal of Inorganic Materials. 25 (12): pp. 1340-1344.
    Source Title
    Wuji Cailiao Xuebao/Journal of Inorganic Materials
    DOI
    10.3724/SP.J.1077.2010.10282
    ISSN
    1000-324X
    School
    Department of Chemical Engineering
    URI
    http://hdl.handle.net/20.500.11937/35520
    Collection
    • Curtin Research Publications
    Abstract

    A nanosized reverse microemulsion reactor was designed for the fabrication of monodispersed SnO2 nanosquares by oxidation of SnF2 under hydrothermal conditions. As-prepared samples were characterized by X-ray diffraction, scanning electron microscope, transmission electron microscope and high resolution transmission electron microscope. The results show that the morphology of the SnO2 nanocrystals can be controlled by regulating the amount of the used oleylamine which direct influenced the pH values of the aqueous phase. Well monodispersed SnO2 nanosquares with the size around 10 nm can be obtained. A proper pH value could benefit the oriented attachments of the crystalline seeds which gradually grew into a square-plate NCs shape in the microemulsion reactor.

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