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    Characterization of Iron III Oxyhydroxides in Hydrometalllurgical Residues

    Access Status
    Fulltext not available
    Authors
    Loan, Mitch
    Richmond, William
    Hockridge, James
    Hart, Robert
    Farrow, John
    Parkinson, Gordon
    St. Pierre, T.
    Newman, M.
    Date
    2005
    Type
    Conference Paper
    
    Metadata
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    Citation
    Loan, Mitch and Richmond, William and Hockridge, James and Hart, Robert and Farrow, John and Parkinson, Gordon and St. Pierre, Timothy G. and Newman, Mike. 2005. : Characterization of Iron III Oxyhydroxides in Hydrometalllurgical Residues, TMS 2005 134th Annual Meeting & Exhibition, 13 Feb, 2005, pp. 13-31. San Francisco, CA: The Minerals, Metals and Materials Society.
    Source Title
    EPD Congress 2005
    Source Conference
    TMS 2005 134th Annual Meeting & Exhibition
    Additional URLs
    http://iweb.tms.org/Purchase/ProductDetail.aspx?Product_code=05-5816-CD
    Faculty
    Division of Engineering, Science and Computing
    Department of Applied Chemistry
    Faculty of Science
    URI
    http://hdl.handle.net/20.500.11937/45922
    Collection
    • Curtin Research Publications
    Abstract

    The characterization of iron iii oxyhydroxides arising from neutralization (removing dissolved iron and/or impurities), or precipitation in storage ponds, mine drainage and waste streams (oxidization of dissoved Fe ii) can prove difficult. The low solubility of iron iii inherently creates a high supersaturation environment favoring the formation of nanoscale, poorly crystalline, and metastable phases. These often have poor physical properties - controlling the properties of the residue - and contain high loadings of important adsorbed components. In this manuscript we provide examples of iron iii oxyhydroxide characterization from hydrometallurgical residues and more synthetic-based studies. We detail techniques to help delineate differences between poorly crystalline iron iii oxyhydroxides (2- and 6-line ferrihydrite, schwertmannite, akaganeite and goethite), and more combinational approaches for when admixed in heterogeneous residues. Generally, identification and even quantification can be achieved with a higher degree of confidence than by use of a single technique such as X-ray diffraction (XRD)

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