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    Fabrication of dense b-calcium orthophosphate with submicrometer-sized grains and its high-temperature superplastic deformation

    Access Status
    Fulltext not available
    Authors
    Watanabe, D.
    Nishio, K.
    Sakka, Y.
    Ohgaki, M.
    Davies, Ian
    Umeda, T.
    Koda, S.
    Itatani, K.
    Date
    2011
    Type
    Journal Article
    
    Metadata
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    Citation
    Watanabe, D. and Nishio, K. and Sakka, Y. and Ohgaki, M. and Davies, I. and Umeda, T. and Koda, S. et al. 2011. Fabrication of dense b-calcium orthophosphate with submicrometer-sized grains and its high-temperature superplastic deformation. Journal of Materials Science. 46: pp. 1956-1962.
    Source Title
    Journal of Materials Science
    ISSN
    00222461
    School
    Department of Mechanical Engineering
    URI
    http://hdl.handle.net/20.500.11937/49469
    Collection
    • Curtin Research Publications
    Abstract

    High-density b-calcium orthophosphate (b-Ca3(PO4)2, also called b-tricalcium phosphate: b-TCP)ceramics with submicrometer-sized grains were fabricated using a pulse-current pressure firing route. The maximum relative density of the b-TCP compacts was 98.7% at 1050 C and this was accompanied by a translucent appearance. The mean grain size of the b-TCP compacts increased slightly with temperature to reach 0.78 lm at 1000 C. However, upon further increasing the firing temperature to 1050 C the mean grain size increased significantly to 1.6 lm. The extent of plastic deformation during tensile testing was examined at temperatures between 900 and 1100 C using a strain rate in the range 9.26 9 10-5 to 4.44 9 10-4 s-1. The maximum tensile strain achieved was 145% for a test temperature of 1000 C and strain rate of 1.48 9 10-4 s-1 and this was attributedto the relatively high density and small grain size.

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