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    A furnace and environmental cell for the in situ investigation of molten salt electrolysis using high-energy X-ray diffraction

    227939.pdf (1.281Mb)
    Access Status
    Open access
    Authors
    Styles, M.
    Rowles, Matthew
    Madsen, I.
    McGregor, K.
    Urban, A.
    Snook, G.
    Scarlett, N.
    Riley, D.
    Date
    2012
    Type
    Journal Article
    
    Metadata
    Show full item record
    Citation
    Styles, M. and Rowles, M. and Madsen, I. and McGregor, K. and Urban, A. and Snook, G. and Scarlett, N. et al. 2012. A furnace and environmental cell for the in situ investigation of molten salt electrolysis using high-energy X-ray diffraction. Journal of Synchrotron Radiation. 19 (1): pp. 39-47.
    Source Title
    Journal of Synchrotron Radiation
    ISSN
    0909-0495
    URI
    http://hdl.handle.net/20.500.11937/5288
    Collection
    • Curtin Research Publications
    Abstract

    This paper describes the design, construction and implementation of a relatively large controlled-atmosphere cell and furnace arrangement. The purpose of this equipment is to facilitate the in situ characterization of materials used in molten salt electrowinning cells, using high-energy X-ray scattering techniques such as synchrotron-based energy-dispersive X-ray diffraction. The applicability of this equipment is demonstrated by quantitative measurements of the phase composition of a model inert anode material, which were taken during an in situ study of an operational Fray-Farthing-Chen Cambridge electrowinning cell, featuring molten CaCl(2) as the electrolyte. The feasibility of adapting the cell design to investigate materials in other high-temperature environments is also discussed.

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