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    3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification

    Access Status
    Fulltext not available
    Authors
    Zhang, L.
    Wu, Changzhi
    Wang, C.
    Zuo, H.
    Shen, Y.
    Date
    2015
    Type
    Journal Article
    
    Metadata
    Show full item record
    Citation
    Zhang, L. and Wu, C. and Wang, C. and Zuo, H. and Shen, Y. 2015. 3,4-Ethylenedioxythiophene functionalizationed with tetrathiafulvalene: Synthesis and selective esterification. Journal of Heterocyclic Chemistry. 51 (5): pp. 1277-1281.
    Source Title
    Journal of Heterocyclic Chemistry
    DOI
    10.1002/jhet.1834
    ISSN
    0022-152X
    School
    Department of Construction Management
    URI
    http://hdl.handle.net/20.500.11937/53921
    Collection
    • Curtin Research Publications
    Abstract

    3,4-(Hydroxymethyl-ethylenedioxy)thiophene (4) and 3,4-(2'-hydroxypropylenedioxy)thiophene (4'') were synthesized from dimethyl 3,4-dihydroxythiophene-2,5-dicarboxylate (1), which were isomers and difficult to separate. When they were esterified with tetrathiafulvalene carried carboxylic acid group, only 3,4-(hydroxymethyl-ethylenedioxy)thiophene (4) could be esterified. No such selectivity was observed when the isomers were esterified by lauric acid and benzoic acid, respectively.

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