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    Emerging surface characterization techniques for carbon steel corrosion: A critical brief review

    Access Status
    Open access via publisher
    Authors
    Dwivedi, D.
    Lepkova, Katerina
    Becker, T.
    Date
    2017
    Type
    Journal Article
    
    Metadata
    Show full item record
    Citation
    Dwivedi, D. and Lepkova, K. and Becker, T. 2017. Emerging surface characterization techniques for carbon steel corrosion: A critical brief review. Proceedings of the Royal Society A. 473 (2199).
    Source Title
    Proceedings of the Royal Society A
    DOI
    10.1098/rspa.2016.0852
    ISSN
    1364-5021
    School
    Department of Chemistry
    URI
    http://hdl.handle.net/20.500.11937/54552
    Collection
    • Curtin Research Publications
    Abstract

    Carbon steel is a preferred construction material in many industrial and domestic applications, including oil and gas pipelines, where corrosion mitigation using film-forming corrosion inhibitor formulations is a widely accepted method. This review identifies surface analytical techniques that are considered suitable for analysis of thin films atmetallic substrates, but are yet to be applied to analysis of carbon steel surfaces in corrosive media or treated with corrosion inhibitors. The reviewed methods include time of flight-secondary ion mass spectrometry, X-ray absorption spectroscopy methods, particleinduced X-ray emission, Rutherford backscatter spectroscopy, Auger electron spectroscopy, electron probe microanalysis, near-edge X-ray absorption fine structure spectroscopy, X-ray photoemission electron microscopy, low-energy electron diffraction, smallangle neutron scattering and neutron reflectometry, and conversion ele ctron Moessbauer spectrometry. Advantages and limitations of the analytical methods in thin-film surface investigations are discussed. Technical parameters of nominated analytical methods are provided to assist in the selection of suitable methods for analysis of metallic substrates deposited with surface films. The challenges associated with the applications of the emerging analytical methods in corrosion science are also addressed.

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