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    Pt nanoparticles supported on nitrogen-doped porous graphene for sensitive detection of Tadalafil

    Access Status
    Fulltext not available
    Authors
    Salah, A.
    Hassan, M.
    Liu, Jian
    Li, M.
    Bo, X.
    Ndamanisha, J.
    Guo, L.
    Date
    2018
    Type
    Journal Article
    
    Metadata
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    Citation
    Salah, A. and Hassan, M. and Liu, J. and Li, M. and Bo, X. and Ndamanisha, J. and Guo, L. 2018. Pt nanoparticles supported on nitrogen-doped porous graphene for sensitive detection of Tadalafil. Journal of Colloid and Interface Science. 512: pp. 379-388.
    Source Title
    Journal of Colloid and Interface Science
    DOI
    10.1016/j.jcis.2017.10.022
    ISSN
    0021-9797
    School
    WASM: Minerals, Energy and Chemical Engineering (WASM-MECE)
    URI
    http://hdl.handle.net/20.500.11937/71549
    Collection
    • Curtin Research Publications
    Abstract

    Graphene (GR) is one of the most promising candidates for utilization in the electroanalytical field because of its superior electrocatalytic activity, excellent electronic conductivity, and high chemical stability. However, the GR sheets usually tend to stack together with p-p interaction. The spontaneous stacking leads to the aggregation of the GR sheets and imposes a negative feedback in the surface area of the GR, which obviously limits its electrochemical application. In this study, nitrogen-doped porous GR (NPGR) with different pore sizes is prepared by using silica (SiO2) as a template. The NPGR exhibits high surface area and porous structure, fulfilling the requirement for supporting materials. Being a support, the structural uniqueness and N dopants of NPGR facilitate the deposition of Pt nanoparticles (Pt NPs). The Pt NPs/NPGR composites integrate the structural properties of NPGR and catalytic properties of Pt NPs. A selective and sensitive electrochemical sensor was successfully developed for sensitive determination of Tadalafil (TAD), showing a concentration range of 1.30–488.9 µM and limit of detection of 0.268 µM.

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