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    Alfred Werner revisited: Some subtleties of complex ion synthesis and isomerism

    19416_19416.pdf (1.041Mb)
    Access Status
    Open access
    Authors
    Ogden, Mark
    Harrowfield, J.
    Skelton, B.
    White, A.
    Date
    2005
    Type
    Journal Article
    
    Metadata
    Show full item record
    Citation
    Harrowfield, Jack M. and Ogden, Mark I. and Skelton, Brian W. and White, Allan H. 2005. Alfred Werner revisited: Some subtleties of complex ion synthesis and isomerism. Comptes Rendus Chimie 8: 121-128.
    Source Title
    Comptes Rendus Chimie
    DOI
    10.1016/j.crci.2004.10.013
    Faculty
    Department of Applied Chemistry
    Division of Engineering, Science and Computing
    Faculty of Science
    Remarks

    NOTICE: this is the author’s version of a work that was accepted for publication in Comptes Rendus Chimie. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Comptes Rendus Chimie, Vol. 8 (2005). DOI: 10.1016/j.crci.2004.10.013

    URI
    http://hdl.handle.net/20.500.11937/8231
    Collection
    • Curtin Research Publications
    Abstract

    The synthesis of perhaps the best-known Wernerian complex, [Co(en)3]3+, is very efficient, but nonetheless results in the formation of various side-products. Today, the use of X-ray crystallography to characterise such materials provides new insights into the reaction pathways of the synthesis and the exact forms possible for the products. The structures of cis-[Co(en)2(H2NCH2CH2NH3)Cl]Cl[ZnCl4], cis-[Co(en)2(NH3)Cl]S2O6, [Co(en)(NH2CH2CH2N=CHCH2NH2))Cl][ZnCl4], [Co(en)2(N-CH3en)][Co(CN)6]?2 H2O and [Co(en)2(N-CH3en)][Co(CN)6], are presently discussed in this regard.

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