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    Synthesis, characterization and adsorptive performance of MgFe2O4 nanospheres for SO2 removal

    Access Status
    Fulltext not available
    Authors
    Zhao, L.
    Li, X.
    Zhao, Q.
    Qu, Z.
    Yuan, D.
    Liu, Shaomin
    Hu, X.
    Chen, G.
    Date
    2010
    Type
    Journal Article
    
    Metadata
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    Citation
    Zhao, Ling and Li, Xinyong and Zhao, Qidong and Qu, Zhenping and Yuan, Deling and Liu, Shaomin and Hu, Xijun and Chen, Guohua. 2010. Synthesis, characterization and adsorptive performance of MgFe2O4 nanospheres for SO2 removal. Journal of Hazardous Materials. 184 (1-3): pp. 704-709.
    Source Title
    Journal of Hazardous Materials
    DOI
    10.1016/j.jhazmat.2010.08.096
    ISSN
    03043894
    School
    Department of Chemical Engineering
    URI
    http://hdl.handle.net/20.500.11937/8819
    Collection
    • Curtin Research Publications
    Abstract

    A type of uniform Mg ferrite nanospheres with excellent SO2 adsorption capacity could be selectively synthesized via a facile solvothermal method. The size of the MgFe2O4 nanospheres was controlled to be 300–400 nm in diameter. The structural, textural, and surface properties of the adsorbent have been fully characterized by a variety of techniques (Brunauer–Emmett–Teller, BET; X-ray diffraction analysis, XRD; scanning electron microscopy, SEM; and energy-dispersive X-ray spectroscopy, EDS). The valence states and the surface chemical compositions of MgFe2O4 nanospheres were further identified by X-ray photoelectron spectroscopy (XPS). The behaviors of SO2 oxidative adsorption on MgFe2O4 nanospheres were studied using Fourier transform infrared spectroscopy (FTIR). Both the sulfite and sulfate species could be formed on the surface of MgFe2O4. The adsorption equilibrium isotherm of SO2 was analyzed using a volumetric method at 298 K and 473 K. The results indicate that MgFe2O4 nanospheres possess a good potential as the solid-state SO2 adsorbent for applications in hot fuel gas desulfurization.

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