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Synthesis and characterisation of 3-vinyl[33](1,2,4) ferrocenophane

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Lu, J.
Baker, M.
Brown, David
Date
2006
Type
Journal Article

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Lu, J. and Baker, M. and Brown, D. 2006. Synthesis and characterisation of 3-vinyl[33](1,2,4) ferrocenophane. Inorganica Chimica Acta. 359: pp. 1299-1302.
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Inorganica Chimica Acta
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Abstract

Treatment of [33](1,2,4)ferrocenophane (1) with N-methylformanilide and phosphorus oxychloride gave 3-formyl[33](1,2,4)ferrocenophane (2) in 96% yield. Subsequently, (2) was reacted with an ylid in THF and 3-vinyl[33](1,2,4)ferrocenophane (3) was obtained in 88% yield.