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    Response Mechanisms and New Approaches with Solid-State Ion-Selective Electrodes: A Powerful Multitechnique Materials Characterization Approach

    Access Status
    Fulltext not available
    Authors
    De Marco, Roland
    Jiang, Zhong-Tao
    Becker, Thomas
    Clarke, Graeme
    Murgatroyd, G.
    Prince, K.
    Date
    2006
    Type
    Journal Article
    
    Metadata
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    Citation
    De Marco, Roland and Jiang, Zhong-Tao and Becker, Thomas and Clarke, Graeme and Murgatroyd, Gareth and Prince, K. 2006. Response Mechanisms and New Approaches with Solid-State Ion-Selective Electrodes: A Powerful Multitechnique Materials Characterization Approach. Electroanalysis 18 (13-14): 1273-1281.
    Source Title
    Electroanalysis
    DOI
    10.1002/elan.200503524
    Faculty
    Department of Applied Chemistry
    Division of Engineering, Science and Computing
    Faculty of Science
    Remarks

    Electroanalysis is available online at: Wiley Interscience

    http://dx.doi.org/10.1002/elan.200503524

    URI
    http://hdl.handle.net/20.500.11937/38274
    Collection
    • Curtin Research Publications
    Abstract

    In modern materials science, there is a plethora of characterization techniques of materials that can provide valuable insights into the fundamental chemical physics of solid-state devices such as chalcogenide glass ion-selective electrodes (ISEs). In this paper, electrochemical impedance spectroscopy (EIS), X-ray photoelectron spectrometry (XPS) and secondary ion mass spectrometry (SIMS) have been used in the elucidation of the mechanistic chemistry of the cadmium chalcogenide glass ISE. Furthermore, in situ synchrotron radiation-grazing incidence X-ray diffraction (SR-GIXRD), in situ EIS/SR-GIXRD, along with small angle neutron scattering (SANS), can be used to unravel the complex relationship between the nanostructure, bulk electrical conductivity and concomitant electrochemical reactivity of an iron chalcogenide glass ISE. Significantly, exciting preliminary modified atomic force microscopy (AFM) data utilizing AFM cantilevers with attached microparticles of the copper sensing material jalpaite demonstrate the tremendous potential of selective force ISE-AFM in the imaging of important molecular structures such as the copper ion channels of cell membranes in fish gills and/or phytoplankton

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