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    In situ high pressure NMR study of the direct synthesis of LiAlH 4

    Access Status
    Fulltext not available
    Authors
    Humphries, Terry
    Birkmire, D.
    Hauback, B.
    McGrady, G.
    Jensen, C.
    Date
    2013
    Type
    Journal Article
    
    Metadata
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    Citation
    Humphries, T. and Birkmire, D. and Hauback, B. and McGrady, G. and Jensen, C. 2013. In situ high pressure NMR study of the direct synthesis of LiAlH 4 . Journal of Materials Chemistry A. 1 (9): pp. 2974-2977.
    Source Title
    Journal of Materials Chemistry A
    DOI
    10.1039/c3ta10239d
    ISSN
    2050-7488
    School
    Department of Physics and Astronomy
    URI
    http://hdl.handle.net/20.500.11937/42615
    Collection
    • Curtin Research Publications
    Abstract

    27Al and 7Li wide-line NMR spectroscopy incorporating a high pressure NMR apparatus has allowed the first in situ study of the solvent mediated, direct synthesis of an alanate, thus overcoming the dearth of analytical techniques available to study phenomena occurring in a pressurised slurry. In contrast to the decomposition reaction, the elucidated hydrogenation pathway does not proceed through the hexahydride intermediate. © 2013 The Royal Society of Chemistry.

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