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dc.contributor.authorHumphries, Terry
dc.contributor.authorBirkmire, D.
dc.contributor.authorHauback, B.
dc.contributor.authorMcGrady, G.
dc.contributor.authorJensen, C.
dc.date.accessioned2017-01-30T15:00:50Z
dc.date.available2017-01-30T15:00:50Z
dc.date.created2015-10-29T04:09:52Z
dc.date.issued2013
dc.identifier.citationHumphries, T. and Birkmire, D. and Hauback, B. and McGrady, G. and Jensen, C. 2013. In situ high pressure NMR study of the direct synthesis of LiAlH 4 . Journal of Materials Chemistry A. 1 (9): pp. 2974-2977.
dc.identifier.urihttp://hdl.handle.net/20.500.11937/42615
dc.identifier.doi10.1039/c3ta10239d
dc.description.abstract

27Al and 7Li wide-line NMR spectroscopy incorporating a high pressure NMR apparatus has allowed the first in situ study of the solvent mediated, direct synthesis of an alanate, thus overcoming the dearth of analytical techniques available to study phenomena occurring in a pressurised slurry. In contrast to the decomposition reaction, the elucidated hydrogenation pathway does not proceed through the hexahydride intermediate. © 2013 The Royal Society of Chemistry.

dc.titleIn situ high pressure NMR study of the direct synthesis of LiAlH 4
dc.typeJournal Article
dcterms.source.volume1
dcterms.source.number9
dcterms.source.startPage2974
dcterms.source.endPage2977
dcterms.source.issn2050-7488
dcterms.source.titleJournal of Materials Chemistry A
curtin.departmentDepartment of Physics and Astronomy
curtin.accessStatusFulltext not available


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