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dc.contributor.authorMoller, Kasper
dc.contributor.authorHansen, B.
dc.contributor.authorDippel, A.
dc.contributor.authorJørgensen, J.
dc.contributor.authorJensen, T.
dc.date.accessioned2018-12-13T09:11:43Z
dc.date.available2018-12-13T09:11:43Z
dc.date.created2018-12-12T02:46:55Z
dc.date.issued2014
dc.identifier.citationMoller, K. and Hansen, B. and Dippel, A. and Jørgensen, J. and Jensen, T. 2014. Characterization of gas-solid reactions using in situ powder X-ray diffraction. Zeitschrift fur Anorganische und Allgemeine Chemie. 640 (15): pp. 3029-3043.
dc.identifier.urihttp://hdl.handle.net/20.500.11937/71898
dc.identifier.doi10.1002/zaac.201400262
dc.description.abstract

© 2014 WILEY-VCH Verlag GmbH & Co. KGaA , Weinheim. X-ray diffraction is a superior technique for structural characterization of crystalline matter. Here we review the use of in situ powder X-ray diffraction (PXD) mainly for real-time studies of solidgas reactions, data analysis and the extraction of valuable knowledge of structural, chemical and physical properties. Furthermore, the diffraction data may also provide knowledge on reaction mechanisms, kinetics and thermodynamic properties. Thus, in situ PXD simultaneously provides properties as a function of pressure, temperature and/ or time at different length scales, i.e. nanoscale structural data and bulk sample properties. Initially, a brief description of experimental and methodological details is provided, followed by a variety of examples of different designs of experiments and methods of data analysis. Additionally, it is discussed how a range of physical properties can be accessed by diffraction techniques, e.g. crystallite size. The aim of this review is to provide new inspiration for utilization of in situ PXD for characterization of a wide range of properties beyond the scope of crystal structure solution.

dc.titleCharacterization of gas-solid reactions using in situ powder X-ray diffraction
dc.typeJournal Article
dcterms.source.volume640
dcterms.source.number15
dcterms.source.startPage3029
dcterms.source.endPage3043
dcterms.source.issn0044-2313
dcterms.source.titleZeitschrift fur Anorganische und Allgemeine Chemie
curtin.departmentSchool of Electrical Engineering, Computing and Mathematical Science (EECMS)
curtin.accessStatusFulltext not available


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