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    Characterization of rutile passivation layers formed on Magnéli-phase titanium oxide inert anodes

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    Access Status
    Open access
    Authors
    Rowles, Matthew
    Scarlett, N.
    Madsen, I.
    McGregor, K.
    Date
    2011
    Type
    Journal Article
    
    Metadata
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    Citation
    Rowles, M. and Scarlett, N. and Madsen, I. and McGregor, K. 2011. Characterization of rutile passivation layers formed on Magnéli-phase titanium oxide inert anodes. Journal of Applied Crystallography. 44 (4): pp. 853-857.
    Source Title
    Journal of Applied Crystallography
    DOI
    10.1107/S0021889811021315
    ISSN
    0021-8898
    URI
    http://hdl.handle.net/20.500.11937/40144
    Collection
    • Curtin Research Publications
    Abstract

    An ex situ characterization study has been performed on rutile passivation layers on inert anodes used for molten salt electrochemical studies. Rutile layer thicknesses were estimated using a number of ex situ methods, including laboratory and synchrotron X-ray diffraction and optical microscopy. The only phases in the anode detected by diffraction were the Magnéli phases (TinO2n-1, n = 5-6) of the unreacted anode and rutile (TiO2), which forms on electrolysis. These measurements validate a previously developed in situ energy-dispersive X-ray diffraction analysis technique [Scarlett, Madsen, Evans, Coelho, McGregor, Rowles, Lanyon & Urban (2009). J. Appl. Cryst. 42, 502-512].

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